Spectrophotometic Determination of some Sulphonamides in Aqueous Solution Via Azo- Dye Formation Reaction

A spectrophotometric method for the determination of trace amounts of some sulphonmides (six compounds) in aqueous solutions is described. The method in based on dizotisation and coupling with pyrogallol to form a yellow coloured, stable and water- soluble azo-dye which shows maximum absorption at 4...

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Bibliographic Details
Main Author: N. Othman (Author)
Format: Book
Published: College of Education for Pure Sciences, 2005-06-01T00:00:00Z.
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Summary:A spectrophotometric method for the determination of trace amounts of some sulphonmides (six compounds) in aqueous solutions is described. The method in based on dizotisation and coupling with pyrogallol to form a yellow coloured, stable and water- soluble azo-dye which shows maximum absorption at 420 nm. Beer's law is obeyed over the concentrations range of 0.4-14 ppm. The relative error is -2.47 to + 3.41 % and the relative standard deviation is ±0.51 to ±2.9% depending on the concentration level. The proposed method has been successfully applied to the determination of sulphacetamide sodium in eye drop drug.
Item Description:1812-125X
2664-2530
10.33899/edusj.2005.81308