Chemical surface modification of lithium disilicate needles of a silica-based ceramic after HF-etching and ultrasonic bath cleaning: impact on the chemical bonding with silane

<p>Recommendations to obtain the best bonding to silica-based ceramics are to prepare its surface by hydrofluoric-acid HF etching and regular application of a silane. This study investigated how the HF-etching followed by ultrasonic water bath cleaning or by an additional phosphoric acid treat...

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Main Authors: A Poulon-Quintin (Author), F Rouzé l'Alzit (Author), E Ogden (Author), A Large (Author), C Bertrand (Author), M Bartala (Author)
Format: Book
Published: Journal of Dental Problems and Solutions - Peertechz Publications, 2022-10-18.
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042 |a dc 
100 1 0 |a A Poulon-Quintin  |e author 
700 1 0 |a  F Rouzé l'Alzit  |e author 
700 1 0 |a  E Ogden  |e author 
700 1 0 |a  A Large  |e author 
700 1 0 |a  C Bertrand  |e author 
700 1 0 |a M Bartala  |e author 
245 0 0 |a Chemical surface modification of lithium disilicate needles of a silica-based ceramic after HF-etching and ultrasonic bath cleaning: impact on the chemical bonding with silane 
260 |b Journal of Dental Problems and Solutions - Peertechz Publications,   |c 2022-10-18. 
520 |a <p>Recommendations to obtain the best bonding to silica-based ceramics are to prepare its surface by hydrofluoric-acid HF etching and regular application of a silane. This study investigated how the HF-etching followed by ultrasonic water bath cleaning or by an additional phosphoric acid treatment impacts the adhesion properties of a resin (G-CEM LinkForce®) with a lithium disilicate glass-ceramic (IPS Emax Press, Ivoclar Vivadent). Comparison is based on results obtained with HF etching and direct silane application. After HF-etching, a water ultrasonic bath (4 minutes), and a final air drying, the scratch test critical load increases (+ 46%) thanks to chemical bonding. Additional tests are presented including heat treatments (at 85 °C before and after silanization). If HF-etching is followed by phosphoric acid treatment and drying of silane at 85 °C, scratch test critical load increases (+ 42%) due to mechanical bonding. Similar adhesion properties are obtained with two opposite protocols. </p> 
540 |a Copyright © A Poulon-Quintin et al. 
546 |a en 
655 7 |a Research Article  |2 local 
856 4 1 |u https://doi.org/10.17352/2394-8418.000115  |z Connect to this object online.