Chemical surface modification of lithium disilicate needles of a silica-based ceramic after HF-etching and ultrasonic bath cleaning: impact on the chemical bonding with silane
<p>Recommendations to obtain the best bonding to silica-based ceramics are to prepare its surface by hydrofluoric-acid HF etching and regular application of a silane. This study investigated how the HF-etching followed by ultrasonic water bath cleaning or by an additional phosphoric acid treat...
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Journal of Dental Problems and Solutions - Peertechz Publications,
2022-10-18.
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LEADER | 00000 am a22000003u 4500 | ||
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001 | peertech__10_17352_2394-8418_000115 | ||
042 | |a dc | ||
100 | 1 | 0 | |a A Poulon-Quintin |e author |
700 | 1 | 0 | |a F Rouzé l'Alzit |e author |
700 | 1 | 0 | |a E Ogden |e author |
700 | 1 | 0 | |a A Large |e author |
700 | 1 | 0 | |a C Bertrand |e author |
700 | 1 | 0 | |a M Bartala |e author |
245 | 0 | 0 | |a Chemical surface modification of lithium disilicate needles of a silica-based ceramic after HF-etching and ultrasonic bath cleaning: impact on the chemical bonding with silane |
260 | |b Journal of Dental Problems and Solutions - Peertechz Publications, |c 2022-10-18. | ||
520 | |a <p>Recommendations to obtain the best bonding to silica-based ceramics are to prepare its surface by hydrofluoric-acid HF etching and regular application of a silane. This study investigated how the HF-etching followed by ultrasonic water bath cleaning or by an additional phosphoric acid treatment impacts the adhesion properties of a resin (G-CEM LinkForce®) with a lithium disilicate glass-ceramic (IPS Emax Press, Ivoclar Vivadent). Comparison is based on results obtained with HF etching and direct silane application. After HF-etching, a water ultrasonic bath (4 minutes), and a final air drying, the scratch test critical load increases (+ 46%) thanks to chemical bonding. Additional tests are presented including heat treatments (at 85 °C before and after silanization). If HF-etching is followed by phosphoric acid treatment and drying of silane at 85 °C, scratch test critical load increases (+ 42%) due to mechanical bonding. Similar adhesion properties are obtained with two opposite protocols. </p> | ||
540 | |a Copyright © A Poulon-Quintin et al. | ||
546 | |a en | ||
655 | 7 | |a Research Article |2 local | |
856 | 4 | 1 | |u https://doi.org/10.17352/2394-8418.000115 |z Connect to this object online. |