Characterization of agarwood incense using gas chromatography - mass spectrometry (GC-MS) coupled with solid phase micro extraction (SPME) and gas chromatography - flame ionization detector (GC-FID) / Nurlaila Ismail ... [et al.]

This paper presents the application of Solid Phase Micro Extraction (SPME) coupled with Gas Chromatography-Mass Spectrometry (GC-MS) and Gas Chromatography-Flame Ionization Detector (GC-FID) to characterize agarwood incense. The work involved three types of SPME fibres at 30 minutes sampling time. T...

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Bibliographic Details
Main Authors: Ismail, Nurlaila (Author), Ibrahim, Mastura (Author), Zareen, Seema (Author), Rahiman, Mohd Hezri Fazalul (Author), Tajuddin, Saiful Nizam (Author), Taib, Mohd Nasir (Author)
Format: Book
Published: Institute of Research Management and Innovation (IRMI), 2015.
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042 |a dc 
100 1 0 |a Ismail, Nurlaila  |e author 
700 1 0 |a Ibrahim, Mastura  |e author 
700 1 0 |a Zareen, Seema  |e author 
700 1 0 |a Rahiman, Mohd Hezri Fazalul  |e author 
700 1 0 |a Tajuddin, Saiful Nizam  |e author 
700 1 0 |a Taib, Mohd Nasir  |e author 
245 0 0 |a Characterization of agarwood incense using gas chromatography - mass spectrometry (GC-MS) coupled with solid phase micro extraction (SPME) and gas chromatography - flame ionization detector (GC-FID) / Nurlaila Ismail ... [et al.] 
260 |b Institute of Research Management and Innovation (IRMI),   |c 2015. 
500 |a https://ir.uitm.edu.my/id/eprint/16086/2/16086.pdf 
520 |a This paper presents the application of Solid Phase Micro Extraction (SPME) coupled with Gas Chromatography-Mass Spectrometry (GC-MS) and Gas Chromatography-Flame Ionization Detector (GC-FID) to characterize agarwood incense. The work involved three types of SPME fibres at 30 minutes sampling time. The fibres are 50/30 jum divinylbenzene-carboxenpolydimethysiloxane (DVB-CAR-PDMS), 65 jum polydi methylsiloxanedivinylbenzene (PDMS-DVB) and 85 jum carboxen-polydimethyl siloxane (CAR-PDMS). The results showed that among many compounds extracted by GC-MS coupled with SPME, six compounds were found significantly presence in high quality agarwood incense due to their high percentage area (%). They are (5-maaliene, ᵝ-elemol, ᵝ-selinene, 10-epi-y-eudesmol, agarospirol and caryophellene oxide. The finding offers a new approach for establishing the volatile profile of agarwood incense components which is beneficial for agarwood grading and discrimination. 
546 |a en 
690 |a Extraction 
655 7 |a Article  |2 local 
655 7 |a PeerReviewed  |2 local 
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