Optimization of headspace solid phase microextraction (HS-SPME) for the extraction of volatile organic compounds (VOCs) in MD2 pineapple / Syaidatul Faraha Zainuddin ... [et al.]
Headspace solid phase microextraction (HS-SPME) was employed for the extraction of volatile organic compounds (VOCs) in MD2 pineapple (Ananas comosus L. var. comosus cv. MD2). Optimisation of HSSPME operating parameters was conducted using three-factor, three-level Box-Behnken response surface exper...
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| Format: | Book |
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Faculty of Applied Sciences,
2020.
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| LEADER | 00000 am a22000003u 4500 | ||
|---|---|---|---|
| 001 | repouitm_47116 | ||
| 042 | |a dc | ||
| 100 | 1 | 0 | |a Zainuddin, Syaidatul Faraha |e author |
| 700 | 1 | 0 | |a Zakaria, Siti Raihan |e author |
| 700 | 1 | 0 | |a Saim, Norashikin |e author |
| 700 | 1 | 0 | |a Dol Hamid, Rossuriati |e author |
| 700 | 1 | 0 | |a Osman, Rozita |e author |
| 245 | 0 | 0 | |a Optimization of headspace solid phase microextraction (HS-SPME) for the extraction of volatile organic compounds (VOCs) in MD2 pineapple / Syaidatul Faraha Zainuddin ... [et al.] |
| 260 | |b Faculty of Applied Sciences, |c 2020. | ||
| 500 | |a https://ir.uitm.edu.my/id/eprint/47116/1/47116.pdf | ||
| 520 | |a Headspace solid phase microextraction (HS-SPME) was employed for the extraction of volatile organic compounds (VOCs) in MD2 pineapple (Ananas comosus L. var. comosus cv. MD2). Optimisation of HSSPME operating parameters was conducted using three-factor, three-level Box-Behnken response surface experimental design to evaluate the interactive effects of temperature (30 - 50 ºC), extraction time (10 - 30 min) and salting effect (1 - 3 g of salt addition) on the amount of selected VOCs. Determination of VOCs was done using gas chromatography with spectrometry detector (GC-MSD). Extraction temperature was found to be significant (p < 0.05) in increasing the amount of selected VOCs (ethyl acetate, methyl isobutyrate and butanoic acid methyl ester). Based on the maximum amount of these VOCs, the optimum operating extraction conditions for HS-SPME were set up at temperature of 30 °C, time of 29 min and salt addition of 1 g. The optimized HS-SPME conditions were employed for the extraction of VOCs from pineapple of different varieties. | ||
| 546 | |a en | ||
| 690 | |a Extraction (Chemistry) | ||
| 690 | |a Pineapple | ||
| 655 | 7 | |a Article |2 local | |
| 655 | 7 | |a PeerReviewed |2 local | |
| 787 | 0 | |n https://ir.uitm.edu.my/id/eprint/47116/ | |
| 856 | 4 | 1 | |u https://ir.uitm.edu.my/id/eprint/47116/ |z Link Metadata |