Preparative isolation of Heteroclitin D from Kadsurae Caulis using normal-phase flash chromatography

• मुख्य लेखकों: Xiao-Xue Yu (लेखक), Qian-Wen Wang (लेखक), Xin-Jun Xu (लेखक), Wei-Jian Lv (लेखक), Ming-Qian Zhao (लेखक), Zhi-Kun Liang (लेखक)
• स्वरूप: पुस्तक
• प्रकाशित: Elsevier, 2013-12-01T00:00:00Z.
• विषय: article
• ऑनलाइन पहुंच: Connect to this object online.

Heteroclitin D (H.D) was successfully isolated from Kadsurae Caulis by using flash chromatography and recrystallized by methanol, 10.2 mg of H.D was obtained from 4.86 g of crude extract, and the purity determined by HPLC was 99.4%. The structure was identified by UV, IR, MS, and NMR analysis. The f...